Influence of ceramic pre-treatments on tensile bond strength and mode of failure of resin bonded to ceramics. 2007

Noéli Boscato, and Alvaro Della Bona, and Altair Antoninha Del Bel Cury
Department of Prosthodontics, School of Dentistry, State University of Campinas, Piracicba, São Paulo, Brazil.

OBJECTIVE To evaluate the effect of ceramic surface treatments on tensile bond strength (sigma) and the mode of failure of a resin bonded to a feldspathic glass and a low-crystalline ceramic, testing the hypothesis that a silica coating treatment is unnecessary for both the glass and the low-crystalline ceramic. METHODS 10 blocks of each the feldspathic glass (V7-VITAVM7) and the leucite-based ceramic (E1-IPS Empress) were fabricated and polished. Five blocks of each ceramic were treated as follows: 9.5% hydrofluoric acid for 60 seconds; and silica coating using Cojet System for 15 seconds. After silane coating, an adhesive resin and a composite were applied and polymerized. The composite-ceramic blocks were cut to produce bar-shaped specimens (n = 30) that were stored in distilled water at 37 degrees C for 7 days before tensile loading to failure in a universal testing machine. Data were statistically analyzed using analysis of variance, Tukey's test (alpha = .01) and Weibull analysis. Fracture surfaces were examined to determine the mode of failure. RESULTS The Weibull modulus (m) and mean sigma value (MPa) of Group E1HF (29.8 +/- 4.5) were significantly higher than other Groups (P = .0001). There was no statistical difference between Groups E1CS (24.6 +/- 5.6) and V7HF (22.3 +/- 4.0). Group V7CS showed the lowest m and mean sigma values (15.7 +/- 6.9) (P = .0001). All fractures occurred within the adhesion zone.

UI MeSH Term Description Entries
D001840 Dental Bonding An adhesion procedure for orthodontic attachments, such as plastic DENTAL CROWNS. This process usually includes the application of an adhesive material (DENTAL CEMENTS) and letting it harden in-place by light or chemical curing. Bonding, Dental,Cure of Orthodontic Adhesives,Curing, Dental Cement,Dental Cement Curing,Orthodontic Adhesives Cure
D003722 Dental Alloys A mixture of metallic elements or compounds with other metallic or metalloid elements in varying proportions for use in restorative or prosthetic dentistry. Alloy, Dental,Alloys, Dental,Dental Alloy
D003764 Dental Materials Materials used in the production of dental bases, restorations, impressions, prostheses, etc. Dental Material,Material, Dental,Materials, Dental
D003776 Dental Porcelain A type of porcelain used in dental restorations, either jacket crowns or inlays, artificial teeth, or metal-ceramic crowns. It is essentially a mixture of particles of feldspar and quartz, the feldspar melting first and providing a glass matrix for the quartz. Dental porcelain is produced by mixing ceramic powder (a mixture of quartz, kaolin, pigments, opacifiers, a suitable flux, and other substances) with distilled water. (From Jablonski's Dictionary of Dentistry, 1992) Porcelain,Porcelain, Dental,Dental Porcelains,Porcelains,Porcelains, Dental
D000538 Aluminum Silicates Any of the numerous types of clay which contain varying proportions of Al2O3 and SiO2. They are made synthetically by heating aluminum fluoride at 1000-2000 degrees C with silica and water vapor. (From Hawley's Condensed Chemical Dictionary, 11th ed) Aluminum Silicate,Silicate, Aluminum,Silicates, Aluminum
D000704 Analysis of Variance A statistical technique that isolates and assesses the contributions of categorical independent variables to variation in the mean of a continuous dependent variable. ANOVA,Analysis, Variance,Variance Analysis,Analyses, Variance,Variance Analyses
D013499 Surface Properties Characteristics or attributes of the outer boundaries of objects, including molecules. Properties, Surface,Property, Surface,Surface Property
D013718 Tensile Strength The maximum stress a material subjected to a stretching load can withstand without tearing. (McGraw-Hill Dictionary of Scientific and Technical Terms, 5th ed, p2001) Strength, Tensile,Strengths, Tensile,Tensile Strengths

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