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Transition-Metal-Free and Oxidant-Free Cross-Coupling of Arylhydrazines with Disulfides: Base-Promoted Synthesis of Unsymmetrical Aryl Sulfides. 2017
Toshihide Taniguchi, and
Takuya Naka, and
Mitsutaka Imoto, and
Motonori Takeda, and
Takeo Nakai, and
Masatoshi Mihara, and
Takumi Mizuno, and
Akihiro Nomoto, and
Akiya Ogawa
Seika Corporation , 1-1-82 Kozaika, Wakayama 641-0007, Japan.
A novel synthesis of unsymmetrical aryl sulfides, which requires no transition metal catalyst and no oxidant, was developed. This base-promoted cross-coupling reaction proceeded using arylhydrazines and 1 equiv amount of disulfides under inert gas conditions to afford the unsymmetrical aryl sulfides in good yields.
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