-transparent.png){kind=logo}
Insights into the Crystallization and Structural Evolution of Glycine Dihydrate by In Situ Solid-State NMR Spectroscopy. 2018
Paolo Cerreia Vioglio, and
Giulia Mollica, and
Marie Juramy, and
Colan E Hughes, and
P Andrew Williams, and
Fabio Ziarelli, and
Stéphane Viel, and
Pierre Thureau, and
Kenneth D M Harris
Aix Marseille Univ, CNRS, ICR, Marseille, France.
In situ solid-state NMR spectroscopy is exploited to monitor the structural evolution of a glycine/water glass phase formed on flash cooling an aqueous solution of glycine, with a range of modern solid-state NMR methods applied to elucidate structural properties of the solid phases present. The glycine/water glass is shown to crystallize into an intermediate phase, which then transforms to the β polymorph of glycine. Our in situ NMR results fully corroborate the identity of the intermediate crystalline phase as glycine dihydrate, which was first proposed only very recently.
| UI | MeSH Term | Description | Entries |
|---|
Related Publications
Paolo Cerreia Vioglio, and
Giulia Mollica, and
Marie Juramy, and
Colan E Hughes, and
P Andrew Williams, and
Fabio Ziarelli, and
Stéphane Viel, and
Pierre Thureau, and
Kenneth D M Harris
February 2015,
Solid state nuclear magnetic resonance,
Paolo Cerreia Vioglio, and
Giulia Mollica, and
Marie Juramy, and
Colan E Hughes, and
P Andrew Williams, and
Fabio Ziarelli, and
Stéphane Viel, and
Pierre Thureau, and
Kenneth D M Harris
July 2022,
The journal of physical chemistry. B,
Paolo Cerreia Vioglio, and
Giulia Mollica, and
Marie Juramy, and
Colan E Hughes, and
P Andrew Williams, and
Fabio Ziarelli, and
Stéphane Viel, and
Pierre Thureau, and
Kenneth D M Harris
November 2017,
Solid state nuclear magnetic resonance,
Paolo Cerreia Vioglio, and
Giulia Mollica, and
Marie Juramy, and
Colan E Hughes, and
P Andrew Williams, and
Fabio Ziarelli, and
Stéphane Viel, and
Pierre Thureau, and
Kenneth D M Harris
November 2022,
Polymers,
Paolo Cerreia Vioglio, and
Giulia Mollica, and
Marie Juramy, and
Colan E Hughes, and
P Andrew Williams, and
Fabio Ziarelli, and
Stéphane Viel, and
Pierre Thureau, and
Kenneth D M Harris
June 2007,
Chemphyschem : a European journal of chemical physics and physical chemistry,
Paolo Cerreia Vioglio, and
Giulia Mollica, and
Marie Juramy, and
Colan E Hughes, and
P Andrew Williams, and
Fabio Ziarelli, and
Stéphane Viel, and
Pierre Thureau, and
Kenneth D M Harris
January 1999,
Biopolymers,
Paolo Cerreia Vioglio, and
Giulia Mollica, and
Marie Juramy, and
Colan E Hughes, and
P Andrew Williams, and
Fabio Ziarelli, and
Stéphane Viel, and
Pierre Thureau, and
Kenneth D M Harris
August 2014,
Angewandte Chemie (International ed. in English),
Paolo Cerreia Vioglio, and
Giulia Mollica, and
Marie Juramy, and
Colan E Hughes, and
P Andrew Williams, and
Fabio Ziarelli, and
Stéphane Viel, and
Pierre Thureau, and
Kenneth D M Harris
July 2008,
The journal of physical chemistry. A,
Paolo Cerreia Vioglio, and
Giulia Mollica, and
Marie Juramy, and
Colan E Hughes, and
P Andrew Williams, and
Fabio Ziarelli, and
Stéphane Viel, and
Pierre Thureau, and
Kenneth D M Harris
August 2011,
The journal of physical chemistry. B,
Paolo Cerreia Vioglio, and
Giulia Mollica, and
Marie Juramy, and
Colan E Hughes, and
P Andrew Williams, and
Fabio Ziarelli, and
Stéphane Viel, and
Pierre Thureau, and
Kenneth D M Harris
November 1997,
Journal of pharmaceutical sciences,
