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Solid-State NMR Spectroscopy: Towards Structural Insights into Starch-Based Materials in the Food Industry. 2022

Mustapha El Hariri El Nokab, and Yasser A Alassmy, and Marwan M Abduljawad, and Khalid M Al-Shamrani, and Mohammed S Alnafisah, and Zahra Asgar Pour, and Chelsea L Tucker, and Khaled O Sebakhy
Zernike Institute for Advanced Materials (ZIAM), University of Groningen, Nijenborgh 4, 9747 AG Groningen, The Netherlands.

Solid-state NMR is a nondestructive and noninvasive technique used to study the chemical structure and dynamics of starch-based materials and to bridge the gap between structure-function relationships and industrial applications. The study of crystallinity, chemical modification, product blending, molecular packing, amylose-amylopectin ratio, end chain motion, and solvent-matrix interactions is essential for tailoring starch product properties to various applications. This article aims to provide a comprehensive and critical review of research characterizing starch-based materials using solid-state NMR, and to briefly introduce the most advanced and promising NMR strategies and hardware designs used to overcome the sensitivity and resolution issues involved in structure-function relationships.

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