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[3 + 2] Cycloaddition of para-Quinone Methides with Nitrile Imines: Approach to Spiro-pyrazoline-cyclohexadienones. 2019
Yingpeng Su, and
Yanan Zhao, and
Bingbing Chang, and
Xiaolong Zhao, and
Rong Zhang, and
Xuan Liu, and
Danfeng Huang, and
Ke-Hu Wang, and
Congde Huo, and
Yulai Hu
College of Chemistry and Chemical Engineering , Northwest Normal University , 967 Anning East Road , Lanzhou 730070 , P. R. China.
[3 + 2] cycloaddition of para-quinone methides with nitrile imines under mild conditions has been achieved. The corresponding spiro-pyrazoline-cyclohexadienone products were constructed in good to excellent yields (up to 97% yield) with high regioselectivity. This straightforward protocol exhibits good functional group tolerance and scalability and provides the spiro-pyrazoline-cyclohexadienones.
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