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Silver-promoted synthesis of vinyl sulfones from vinyl bromides and sulfonyl hydrazides in water. 2020
Ge Zhang, and
Jian-Guo Fu, and
Qian Zhao, and
Gui-Shan Zhang, and
Meng-Yao Li, and
Chen-Guo Feng, and
Guo-Qiang Lin
School of Physical Science and Technology, ShanghaiTech University, Shanghai, 201210, China.
The synthesis of vinyl sulfones via silver-promoted cross-coupling of vinyl bromides with sulfonyl hydrazides was realized. Water was used as the sole solvent. Multisubstituted vinyl sulfones were easily prepared with excellent alkyl group tolerance. A mechanism involving nucleophilic attack of a sulfinate anion was proposed.
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