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Solvent- and transition metal-free amide synthesis from phenyl esters and aryl amines. 2019
Sergey A Rzhevskiy, and
Alexandra A Ageshina, and
Gleb A Chesnokov, and
Pavel S Gribanov, and
Maxim A Topchiy, and
Mikhail S Nechaev, and
Andrey F Asachenko
A.V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences Leninsky Prospect 29 Moscow 119991 Russia aasachenko@ips.ac.ru.
A general, economical, and environmentally friendly method of amide synthesis from phenyl esters and aryl amines was developed. This new method has significant advantages compared to previously reported palladium-catalyzed approaches. The reaction is performed transition metal- and solvent-free, using a cheap and environmentally benign base, NaH. This approach enabled us to obtain target amides in high yields with high atom economy.
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