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Visible light-enabled synthesis of phosphorylated indolizine and pyridoindole derivatives via HAT-mediated radical cascade cyclization. 2023
Kunrong Shen, and
Chuan Feng, and
Yilei Liu, and
Dong Yi, and
Peng Lin, and
Huifang Li, and
Yimou Gong, and
Siping Wei, and
Qiang Fu, and
Zhijie Zhang
Green Pharmaceutical Technology Key Laboratory of Luzhou City, Central Nervous System Drug Key Laboratory of Sichuan Province, School of Pharmacy, Southwest Medical University, Luzhou, 646000, China. zzj30@swmu.edu.cn.
A visible light-enabled cascade cyclization strategy is disclosed with concomitant phosphorylation and heterocycle construction. It provides a novel and environmentally benign approach for accessing tetrahydroindolizine-containing phosphonates under metal-free conditions. Mechanistic studies revealed that phosphinoyl radicals were generated from H-phosphonates via a HAT process.
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