Liquid chromatographic determination of benzoic acid in orange juice: interlaboratory study. 1995

H S Lee
Florida Department of Citrus, Citrus Research and Education Center, Lake Alfred 33850.

An interlaboratory study was carried out for the determination of benzoic acid in orange juice by liquid chromatography. The orange juice was fortified with 0.5-10 ppm benzoic acid. Statistical analysis of the results showed that relative reproducibility (RSDR) between laboratories ranged from 6.92 to 15.97% for juice fortified with 1-10 ppm benzoic acid; RSDR was 27.90% for juice fortified with 0.5 ppm benzoic acid. Mean recoveries ranged from 94.5% for 4 ppm benzoic acid to 114% for 0.5 ppm benzoic acid. Total variability increased with increasing fortification level as measured by standard deviation for reproducibility (SR).

UI MeSH Term Description Entries
D007202 Indicators and Reagents Substances used for the detection, identification, analysis, etc. of chemical, biological, or pathologic processes or conditions. Indicators are substances that change in physical appearance, e.g., color, at or approaching the endpoint of a chemical titration, e.g., on the passage between acidity and alkalinity. Reagents are substances used for the detection or determination of another substance by chemical or microscopical means, especially analysis. Types of reagents are precipitants, solvents, oxidizers, reducers, fluxes, and colorimetric reagents. (From Grant & Hackh's Chemical Dictionary, 5th ed, p301, p499) Indicator,Reagent,Reagents,Indicators,Reagents and Indicators
D002853 Chromatography, Liquid Chromatographic techniques in which the mobile phase is a liquid. Liquid Chromatography
D002957 Citrus A plant genus of the family RUTACEAE. They bear the familiar citrus fruits including oranges, grapefruit, lemons, and limes. There are many hybrids which makes the nomenclature confusing. Citron Tree,Fruit, Citrus,Lemon Tree,Orange Tree, Bitter,Orange Tree, Mandarin,Orange Tree, Seville,Orange Tree, Sour,Pomelo Tree,Pummelo Tree,Tangerine Tree,Citrus Fruit,Citrus aurantium,Citrus bergamia,Citrus grandis,Citrus hystrix,Citrus limon,Citrus maxima,Citrus medica,Citrus reticulata,Kaffir Lime,Bitter Orange Tree,Bitter Orange Trees,Citron Trees,Citrus aurantiums,Citrus bergamias,Citrus grandi,Citrus hystrices,Citrus medicas,Citrus reticulatas,Lemon Trees,Lime, Kaffir,Mandarin Orange Tree,Mandarin Orange Trees,Orange Trees, Bitter,Orange Trees, Mandarin,Orange Trees, Seville,Orange Trees, Sour,Pomelo Trees,Pummelo Trees,Seville Orange Tree,Seville Orange Trees,Sour Orange Tree,Sour Orange Trees,Tangerine Trees,Tree, Bitter Orange,Tree, Citron,Tree, Lemon,Tree, Mandarin Orange,Tree, Pomelo,Tree, Pummelo,Tree, Seville Orange,Tree, Sour Orange,Tree, Tangerine,Trees, Bitter Orange,Trees, Citron,Trees, Lemon,Trees, Mandarin Orange,Trees, Pomelo,Trees, Pummelo,Trees, Seville Orange,Trees, Sour Orange,Trees, Tangerine,aurantium, Citrus,bergamia, Citrus,hystrices, Citrus,maxima, Citrus,medicas, Citrus,reticulata, Citrus
D005374 Filtration A process of separating particulate matter from a fluid, such as air or a liquid, by passing the fluid carrier through a medium that will not pass the particulates. (McGraw-Hill Dictionary of Scientific and Technical Terms, 4th ed) Filtrations
D005520 Food Preservatives Substances capable of inhibiting, retarding or arresting the process of fermentation, acidification or other deterioration of foods. Preservatives, Food
D001565 Benzoates Derivatives of BENZOIC ACID. Included under this heading are a broad variety of acid forms, salts, esters, and amides that contain the carboxybenzene structure. Benzoate,Benzoic Acids,Acids, Benzoic
D001628 Beverages Liquids that are suitable for drinking. (From Merriam Webster Collegiate Dictionary, 10th ed) Beverage
D019817 Benzoic Acid A fungistatic compound that is widely used as a food preservative. It is conjugated to GLYCINE in the liver and excreted as hippuric acid. Potassium Benzoate,Ucephan,Acid, Benzoic,Benzoate, Potassium

Related Publications

H S Lee
December 2013, Se pu = Chinese journal of chromatography,
H S Lee
January 1977, Journal - Association of Official Analytical Chemists,
H S Lee
January 1989, Journal - Association of Official Analytical Chemists,
H S Lee
January 1989, Journal - Association of Official Analytical Chemists,
H S Lee
January 1988, Journal - Association of Official Analytical Chemists,
Copied contents to your clipboard!