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Rhodium(III)-Catalyzed C(sp3)-H Bond Aminocarbonylation with Isocyanates. 2018
Huaiqing Zhao, and
Xi Zhou, and
Bo Li, and
Xiufen Liu, and
Ningxin Guo, and
Zhengliang Lu, and
Shoufeng Wang
Key Laboratory of Interfacial Reaction & Sensing Analysis in Universities of Shandong, School of Chemistry and Chemical Engineering , University of Jinan , Jinan , Shandong , 250022 , P. R. China.
Rh(III)-catalyzed C(sp3)-H bond aminocarbonylation of 8-methylquinolines and isocyanates has been realized under mild conditions. This approach is applicable to different aryl and alkyl isocyanates, leading to the synthesis of various α-quinolinyl amide compounds in moderate to excellent yields. A plausible mechanism for this transformation is proposed according to the experimental results obtained.
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