Partial purification and some properties of beta-phosphoglucomutase from Lactobacillus brevis. 1984

L R Marechal, and G Oliver, and L A Veiga, and A A de Ruiz Holgado

A phosphoglucomutase (beta-phosphoglucomutase) specific for beta-glucose 1-phosphate, which catalyzes the beta-glucose 1-phosphate:glucose 6-phosphate interconversion, was 560-fold purified from Lactobacillus brevis strain L6. The isoelectric point of beta-phosphoglucomutase was 3.8 and it had an apparent molecular weight of 29,000 estimated by gel chromatography. The enzyme required a divalent cation (Mn2+ greater than Mg2+ greater than Ni2+ greater than Co2+) and beta-glucose 1,6-bisphosphate for activity. The equilibrium constant Ke for the reaction beta-D-glucose 1-phosphate in equilibrium D-glucose 6-phosphate at 30 degrees C and pH 6.7 is 18.5. beta-phosphoglucomutase had a pH optimum between 6.3 and 6.8 and appeared to be quite specific: alpha-glucose 1-phosphate, alpha- or beta-galactose 1-phosphate and alpha- or beta-N-acetylglucosamine 1-phosphate did not substitute for beta-glucose 1-phosphate. Double reciprocal plots of the data from initial velocity studies at five beta-glucose 1-phosphate concentrations (10 to 100 microM) and four beta-glucose 1,6-bisphosphate concentrations (0.125 to 1.0 microM) showed that the apparent Michaelis constants for beta-glucose 1-phosphate and beta-glucose 1,6-bisphosphate were related to the concentrations of beta-glucose 1,6-bisphosphate and beta-glucose 1-phosphate, respectively, in such a way as to suggest a ping-pong mechanism. The same conclusion was obtained when substrate-velocity relationships were investigated at fixed ratio of both substrates: the Lineweaver-Burk plots showed linear lines and no parabolic ones. The "true" Km for beta-glucose 1-phosphate and beta-glucose 1,6-bisphosphate were found to be about 12 and 0.8 microM, respectively.

UI MeSH Term Description Entries
D007700 Kinetics The rate dynamics in chemical or physical systems.
D007778 Lactobacillus A genus of gram-positive, microaerophilic, rod-shaped bacteria occurring widely in nature. Its species are also part of the many normal flora of the mouth, intestinal tract, and vagina of many mammals, including humans. Lactobacillus species are homofermentative and ferment a broad spectrum of carbohydrates often host-adapted but do not ferment PENTOSES. Most members were previously assigned to the Lactobacillus delbrueckii group. Pathogenicity from this genus is rare.
D010733 Phosphoglucomutase An enzyme that catalyzes the conversion of alpha D-glucose 1-phosphate to alpha D-glucose 6-phosphate. EC 5.4.2.2. Glucose Phosphomutase,Phosphomutase, Glucose
D002384 Catalysis The facilitation of a chemical reaction by material (catalyst) that is not consumed by the reaction. Catalyses
D002621 Chemistry A basic science concerned with the composition, structure, and properties of matter; and the reactions that occur between substances and the associated energy exchange.
D004789 Enzyme Activation Conversion of an inactive form of an enzyme to one possessing metabolic activity. It includes 1, activation by ions (activators); 2, activation by cofactors (coenzymes); and 3, conversion of an enzyme precursor (proenzyme or zymogen) to an active enzyme. Activation, Enzyme,Activations, Enzyme,Enzyme Activations
D055598 Chemical Phenomena The composition, structure, conformation, and properties of atoms and molecules, and their reaction and interaction processes. Chemical Concepts,Chemical Processes,Physical Chemistry Concepts,Physical Chemistry Processes,Physicochemical Concepts,Physicochemical Phenomena,Physicochemical Processes,Chemical Phenomenon,Chemical Process,Physical Chemistry Phenomena,Physical Chemistry Process,Physicochemical Phenomenon,Physicochemical Process,Chemical Concept,Chemistry Process, Physical,Chemistry Processes, Physical,Concept, Chemical,Concept, Physical Chemistry,Concept, Physicochemical,Concepts, Chemical,Concepts, Physical Chemistry,Concepts, Physicochemical,Phenomena, Chemical,Phenomena, Physical Chemistry,Phenomena, Physicochemical,Phenomenon, Chemical,Phenomenon, Physicochemical,Physical Chemistry Concept,Physicochemical Concept,Process, Chemical,Process, Physical Chemistry,Process, Physicochemical,Processes, Chemical,Processes, Physical Chemistry,Processes, Physicochemical

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